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Two new organically templated borates, [(1,10-phen)(H 3 BO 3 ) 2 ] ( 1 ) and [2-EtpyH][(B 5 O 6 (OH) 4 ] ( 2 ), were synthesized under mild solvothermal conditions and characterized by single-crystal X-ray diffraction, FT-IR, elemental analyses and thermogravimetry. Complex  1  is a co-crystal component in which B(OH) 3  molecules form crinkled tapes via hydrogen bonds, which in turn are packed in a two-dimensional framework with 1,10-phen molecules sandwiched between the framework of crinkled chains. The structure of complex  2  is composed of 2-ethylpyridinium cations [2-EtpyH] +  and pentaborate anions [B 5 O 6 (OH) 4 ] –  which are linked together with hydrogen bonds to form a three-dimensional supramolecular framework. The templating [2-EtpyH] +  cations are situated in the cavities arising from the supramolecular pentaborate framework and interact also with the inorganic framework through hydrogen bonds.

zeitschrift für naturforschung b

Hydrogen-bonded assemblies of two organically templated borates: syntheses and crystal structures of [(1,10-phen)(H 3 BO 3 ) 2 ] and [2-EtpyH][(B 5 O 6 (OH) 4 ]