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The reaction of Cu(II) nitrate with sodium 2-chlorobenzoate (NaL 1 ) and ( E )-1,2-di(pyridin-4-yl)ethene (dpe) yields a new complex [Cu(L 1 ) 2 (dpe)(H 2 O)] ( 1 ). When Zn(II) nitrate reacts with sodium 4-chlorobenzoate (NaL 2 ) and 1,2-di(pyridin-4-yl)ethane (dpa), [Zn(L 2 ) 2 (dpa)]·CH 3 OH ( 2 ) is obtained. Complexes  1  and  2  have been characterized by single-crystal X-ray diffraction, IR spectroscopy, and elemental and thermogravimetric analyses.  1  shows a 3D CdS network structure with uninodal 4-connected (6 5 .8) topology; complex  2  displays a chain structure.

Syntheses and structural characterization of coordination polymers of Cu(II) and Zn(II) chlorobenzoates and bis(pyridin-4-yl)-substituted species