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A salt with the composition [C 12 H 9 N 2 ][C 8 H 3 Cl 2 O 4 ] (1) with 4,5-dichlorophthalic acid and 1,10- phenanthroline (phen) has been synthesized and characterized by IR, UV spectroscopy, elemental analysis, and X-ray crystallography. Compound 1 represents a 3D chiral supramolecular framework containing monohelical chains (2 1  axis) through multiform C-H· · ·O, O-H· · · O, N-H· · ·N intramolecular hydrogen bonds and C-H· · ·O, N-H· · ·O intermolecular hydrogen bonds. Otherwise, two types of face-to-face π · · ·π interactions between the aromatic rings are found in the solid state. The luminescent properties of compound 1 were investigated in the solid state at room temperature

A 3D Chiral Hydrogen Bond Framework Based on Phenanthrolinium Hydrogen 4,5-Dichlorophthalate: Crystal Structure and Luminescent Properties