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Colorless needles of Ga 2−x Sc x O 3  (x = 0.83) were isolated during the crystal growth of La 3 Ga 3 Sc 2 O 12  in a K 2 WO 4  flux. The structure was refined from X-ray single-crystal data: β -Ga 2 O 3  type,C2/m, Z = 4, a = 12.716(4), b = 3.1566(6), c = 5.928(5) Å , β = 102.57(3)◦,V = 232.2 Å3, wR2 = 0.0618, 429 F 2  values, 32 variables. The structure is based on infinite double chains of edge-sharing Sc/GaO 6  octahedra running along the b axis. The GaO 4  tetrahedra connect these chains by sharing corners and form a three-dimensional framework. The oxygen atoms form a distorted ccp pattern. The  45 Sc NMR spectra confirm the presence of a single scandium site, while  71 Ga NMR data clearly prove the partial occupancy of the scandium site by gallium atoms. The nuclear electric quadrupolar parameters of  45 Sc and  71 Ga are discussed in relation to the crystallographic atomic environments

Single-crystal Structure and Solid-state NMR of Ga 2–x Sc x O 3 (x = 0.83)