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The reaction of the diimine ligand 1,2-bis(1,3-diisopropyl-4,5-dimethylimidazolin-2-imino)ethane (BL iPr ) with tetrameric [Cp*RuCl] 4  in a 1 : 0.75 ratio afforded the complex salt [1][2] containing the 16-electron half-sandwich cation [Cp*Ru(BL iPr )]+ (1) and the dinuclear anion [Cp*Ru(μ- Cl) 3 RuCp*] −  (2). The X-ray crystal structures of [1][2]·31/2THF (monoclinic, space group P2 1 /n, Z = 4) and of [1][2]·THF (monoclinic, space group C2/m, Z = 4) are reported, allowing the structural characterization of the unprecedented anion 2, in which two [(η 5 -C 5 Me 5 )Ru(II)] moieties are bridged by three μ 2 -chlorine atoms.

zeitschrift für naturforschung b

Structural Characterization of Cationic 16-Electron Pentamethylcyclopentadienyl Ruthenium(II) Complexes Containing the Binuclear [Cp*Ru(μ-Cl)3RuCp*]– Anion