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New methano[1,5]dioxocines, O-heterocycles with a framework similar to Tröger’s base, were prepared by means of a three-component reaction. The scope of this domino reaction was studied.

Synthesis of New Methano[1,5]dioxocines via a Domino Reaction of 4-Hydroxy-2H-pyran-2-ones / 4-Hydroxy-2H-chromen-2-ones with Acyclic 1,3-Diketones