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The compounds β -RE(BO 2 ) 3  [RE = Nd (neodymium meta-borate), Sm (samarium meta-borate) and Gd (gadolinium meta-borate)] were synthesized under high-pressure and high-temperature conditions in a Walker-type multianvil apparatus at 3.5 GPa (Nd), 7.5 GPa (Sm, Gd) and 1050 °C. The crystal structures were determined by single crystal X-ray diffraction data collected at r. t. (Sm, Gd) and at−73°C (Nd), respectively. The structures are isotypic with the already known ambient-pressure phases β -RE(BO 2 ) 3  (RE = (Tb, Dy) and the high-pressure phases β -RE(BO 2 ) 3  (RE = Ho-Lu)

High-Pressure Syntheses, Crystal Structures, And Thermal Behaviour Of β-Re(Bo 2 ) 3 (Re = Nd, Sm, Gd)