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The title compounds are formed by reaction of Dyl 3 , Dy metal and C in stoichiometric amounts in closed Ta ampoules, Dy 10 (C 2 ) 2 I 18   at 930 °C 7days, Dy 4  (C 2 )I 6  at 950 °C for 6 days and Dy 12 (C 2 ) 3 I 17  at 900 °C for 11 days as pure samples according to X-ray powder diffraction. Dy 10 (C 2 ) 2 I 18  crystallizes in space group P2 1/c  with a = 10.470(2), b = 17.152(3), c = 13.983(3) Å and β = 121.14(3)°, Dy 4 (C 2 )I 6  in Pnnm with a = 13.622(3), b = 14.335(3) and c = 8.396(2) Å , and Dy 12 (C 2 ) 3 I 17  in C2/c with a = 19.149(4), b = 12.069(2), c = 18.595(4) Å , and β = 90.54(3)°. The crystal structure of Dy 10 (C 2 ) 2 I 18  is composed of Dy double octahedra centered by (C2) 6−  groups (ethanide) with the iodide ions above the edges and the corners of the Dy 10 (C 2 )2 units. In Dy 4 (C 2 )I 6  the Dy atoms form chains of trans-edge sharing octahedra with embedded (C 2 ) groups. In the structure of Dy 12 (C 2 ) 3 I 17  alternately cis-, trans-edge-condensed Dy 6  octahedra centered by (C 2 ) groups occur. The iodine atoms surround the chains like in the M 6 X 12  cluster and interconnect neighboring chains.

zeitschrift für naturforschung b

Dysprosiumcarbidiodide Dy 10 (C 2 ) 2 I 18 , Dy 4 (C 2 )I 6  und Dy 12 (C 2 ) 3 I 17  / Dysprosium Carbide Iodides Dy 10 (C 2 ) 2 I 18 , Dy 4 (C 2 )I 6 , and Dy 12 (C 2 ) 3 I 17