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Crystals of [Me 4 N] 2 [HgI 4 ] (1) and [Me 4 N][Hg 2 I 5 ] (2), were obtained from solutions of stoichiometric amounts of HgI 2  and Me 4 NI in EtOH or acetone, resp., while crystals of [Li(12-crown- 4) 2 ] 2 [Hg 4 I 10 ] (3) formed upon interdiffusion of methanolic solutions of HgI 2 , LiI and of the auxiliary ligand. The crystal structures of the compounds were determined. The [Hg 2 I 5 ]− ion in (2) has a polymeric sheet structure, built up from [Hg 2 I 6 ] units bridged by [HgI 4 ] groups sharing common apices. The [Hg 4 I 10 ] 2−  ion in 3 consists of four [HgI 4 ] tetrahedra sharing common edges. A short survey on the iodomercurate(II) anions known up to now is given and a classification is proposed

zeitschrift für naturforschung b

Untersuchungen Über Iodomercurate: Kristallstrukturen Von Bis-Tetramethylammonium-Tetraiodomercurat(Ii), Tetramethylammoniumpentaiododimercurat(Ii) Und Bis[Di(12-Krone-4)Lithium]-Decaiodotetramercurat(Ii)