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The complex [Ni(pn) 3 ][Fe(CN) 5 NO]·H 2 O (1) was synthesised by the reaction of [Ni(pn) 3 ]Cl 2  (pn = racemic propane-1,2-diamine) with Na 2 [Fe(CN) 5 NO]·2H 2 O in aqueous solution and has been charaterised by IR and Mössbauer spectroscopy and magnetic studies. Single crystal structure analysis revealed octahedrally coordinate cations [Ni(pn) 3 ] 2+  and anions [Fe(CN) 5 NO] 2− .

Synthesis, Characterisation, Structure, and Magnetic Properties of [Ni{H 2 NCH(CH 3 )CH 2 NH 2 } 3 ][Fe(CN) 5 NO]·H 2 O