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New zinc(II) and cadmium(II) complexes of the 2,2’-diamino-4,4’-bithiazole (DABTZ) ligand, [M(DABTZ) 2 (CH 3 COO)](ClO 4 ), have been synthesized and characterized by elemental analysis, IR, 1H NMR and 13C NMR spectroscopy. The structural characterization of the Cd(DABTZ) 2 (CH 3 COO)](ClO 4 ) · 2H 2 O complex shows the complex to be a monomer and the Cd atom to be coordinated by four nitrogen atoms of the “DABTZ” ligands and two oxygen atoms of the acetate anion. There is an edge-to-edge π-π stacking interaction between the parallel aromatic rings.

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Syntheses and Characterization of Two New 4,4’-Bithiazole d 10  Complexes, Structural Characterization of M(DABTZ) 2 (CH 3 COO)](ClO 4 ) · 2H 2 O (M = Zn, Cd)