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Starting from 4,5-(ethylenedithio)-1,3-dithiol-2-one and 1,3-dithiol-2-one the disodium 5,6-dihydro-1,4-dithiin-2,3- dithiolate (Na 2 dddt) and disodium 1,2-dithiolate (Na 2 edt) salts were prepared, which react with NiCl 2  in air to give the complex Ni(dddt)(edt) (3ab). This compound was characterized analytically and spectroscopically. The method is applicable for the preparation of similar unsymmetrical complexes.

zeitschrift für naturforschung b

Alternative Method for the Preparation of Ni(dddt)(edt) (dddt = 5,6-Dihydro- 1,4-dithiin-2,3-dithiolate, edt = cis-1,2- Ethylenedithiolate) and Similar Complexes