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A new silver(I) nitrate complex of 2-(2-aminoethyl)pyridine (aepy), [Ag 2 (μ-NO 3 ) 2 (μ-aepy) 2 ] n , has been synthesized and characterized by elemental analysis, IR spectroscopy and single crystal X-ray diffractometry. Two silver(I) ions are doubly bridged by two bidentate aepy ligands forming dimeric building block [Ag 2 (μ-aepy) 2 ] units with a Ag···Ag distance of 3.0587(17)Å . These dimeric units are further doubly bridged by two nitrato ligands into a one-dimensional polymeric chain. The nitrato ligand exhibits an uncommon bidentate bridging mode of Ag-ONO-Ag. The title complex features a hydrogen bonded two-dimensional supramolecular framework formed via N-H···O hydrogen bonds, involving the uncoordinated O atom of the nitrate ligand and amine hydrogen atoms of aepy. The thermal stability of the title complex was investigated using thermogravimetry and differential thermal analysis.

A New One-Dimensional Coordination Polymer of Silver(I) with Bridging 2-(2-Aminoethyl)pyridine and Nitrato Ligands: [Ag 2 (μ–NO 3 ) 2 (μ–aepy) 2 ] n