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Cobalt(II) and zinc(II) complexes of ethyl carbazate (ECZ), [Co(ECZ) 3 ](NO 3 ) 2  and [Zn(ECZ) 3 ] (NO 3 ) 2 , were synthesized. Single crystals of these two compounds were grown from aqueous solutions using a slow evaporation method. Their structures have been determined by X-ray diffraction analysis. Both of them are monoclinic with space group P2 1 /n. The complexes are further characterized by element analysis and IR measurements. Their thermal stabilities are studied by using TG-DTG, DSC techniques. When heated to 350 °C, only metal oxide was left for both complexes.

Syntheses, Crystal Structures and Thermal Stability of Co(II) and Zn(II) Complexes with Ethyl Carbazate