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Cobalt orotate trihydrate, [Co(C 5 N 2 O 4 H 2 )]·3H 2 O, has been synthesized and its crystal structure determined. The title compound crystallizes in the orthorhombic space group P2 1 2 1 2 1  (no. 19) with a = 771.5(2), b = 788.9(7), c = 1470.4(2) pm, and Z = 4. Bridging orotate anions coordinate in a mono- and bidentate manner to the Co atom resulting in infinite chains of alternating Co(II) cations and orotate (OrH 2− ) anions parallel to the c axis. The distorted octahedral Co coordination geometry is completed by three H 2  molecules. The FT-Raman and FT-IR spectra of the crystalline compound have been recorded and an assignment of the vibrational modes is proposed. The thermal behavior (TG) was investigated.

Synthesis, Crystal Structure and Vibrational Spectrum of Cobalt(II)orotate Trihydrate, [Co(C 5 N 2 O 4 H 2 ) · 3 H 2 O