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The tetrakis(phenyl isocyanide)nickel(0) complexes [Ni(CNR) 4 ](R = C 6 H 5 , 1; R= C 6 H 3 -2,6-Me 2 , 2; R = C 6 H 4 -2-NO 2 , 3) have been synthesized from [Ni(COD) 2 ] and the corresponding phenyl isocyanides in toluene. Complexes 1 - 3 were characterized by X-ray diffraction. All three complexes contain a nickel atom which is coordinated in a slightly distorted tetrahedral fashion.

Homoleptic Nickel(0) Phenyl Isocyanide Complexes