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Treatment of the dilithiated dibenzotetraethyleneglycol reagent [(o-C 6 H 4 OLi)-(OCH 2 CH 2 ) 2 O- (o-C 6 H 4 OLi)] (5) with TiCl 4  · 2 THF gave the corresponding metal complex [{(o-C 6 H 4 O-) - (OCH 2 CH 2 ) 2 O-(o-C 6 H 4 O-)}TiCl 2 ] (6). The X-ray crystal structure analysis of 6 revealed that all five oxygen atoms are located in one plane and bonded to titanium in a pentagonal-dipyramidal geometry with the two chloride ligands being oriented trans to each other in the apical positions.

An Internally Coordinated Metalla[14]-crown-5 System with a Pentagonal-dipyramidal Coordination Geometry of the Central Titanium Atom