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Crystals of K 2 Pt(CN) 4 Br 2 , K 2 Pt(CN) 4 I 2  and K 2 Pt(CN) 4 Cl 2  ·2H 2 O were grown, and their crystal structures have been determined from single crystal data. The structure of K 2 Pt(CN) 4 Cl 2  has been determined and refined from X-ray powder data. All compounds crystallize monoclinicly (P2 1 /c; Z = 2), and K 2 Pt(CN) 4 X 2  with X = Cl, Br, I are isostructural. K 2 Pt(CN) 4 Cl 2 : a = 708.48(2); b = 903.28(3); c = 853.13(3) pm; β = 106.370(2)°; R p  = 0.064 (N(hkl) = 423). K 2 Pt(CN) 4 Br 2 : a = 716.0(1); b = 899.1(1); c = 867.9(1) pm; β = 106.85(1)°; R(F) N′  = 0.026 (N’(hkl) = 3757). K 2 Pt(CN) 4 I 2 : a = 724.8(1); b = 914.5(1); c = 892.1(1) pm; β = 107.56(1)°; R(F) N′  = 0.025 (N’(hkl) = 2197). K 2 Pt(CN) 4 Cl 2   ·2H2O: a = 763.76(4); b = 1143.05(6); c = 789.06(4) pm; β = 105.18(1)°; R(F) N′  = 0.021 (N’(hkl) = 2281). Raman and infrared spectroscopy data are reported.

zeitschrift für naturforschung b

Kristallzucht und Strukturaufklärung von K 2 [Pt(CN) 4 Cl 2 ], K 2 [Pt(CN) 4 Br 2 ], K 2 [Pt(CN) 4 I 2 ] und K 2 [Pt(CN) 4 Cl 2 ] · 2H 2 O/ Crystal Growth and Crystal Structure Determination of K 2 [Pt(CN) 4 Cl 2 ], K 2 [Pt(CN) 4 Br 2 ], K 2 [Pt(CN) 4 I 2 ] and K 2 [Pt(CN) 4 ]Cl 2 ] · 2H 2 O