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Triethoxysilane HSi(OEt) 3 , tetraethoxysilane Si(OEt) 4  and hexaethoxydisiloxane Si 2 O(OEt) 6  have been probed as reagents for the synthesis of hydrogen-rich silyl-arenes Ar(SiH 3 ) n . A large set of new silyl-arenes, varying in their substitution patterns and grades, have been prepared. The results establish the two new silylating agents HSi(OEt) 3  and Si 2 O(OEt) 6  as particularly useful alternatives to Si(OEt) 4 . The products, which include trihydrosilyl-substituted methylbenzenes, naphthalenes and ferrocenes, have been characterized by NMR and IR spectroscopy, mass spectrometry and single crystal X-ray diffraction.

Triethoxysilane, Tetraethoxysilane and Hexaethoxydisiloxane – Three Complementary Reagents for the Synthesis of Hydrogen-Rich Silylarenes