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Single crystals of potassium hydrogenphthalate monohydrate, KHPhth(H 2 O), were grown from aqueous solution using a slow cooling method and the structure was determined by X-ray diffraction analysis. The crystals belong to the monoclinic space group P2 1 /c. Its unit cell parameters are as follows: a = 1.1235(1), b = 0.6689(1), c = 1.1998(2) nm, β = 98.85°, V = 0.8909(1) nm 3 , Dc = 1.657 g/cm 3 , Z = 4, F(000) = 456. The thermal decomposition of the complex was studied using differential scanning calorimetry (DSC), thermogravimetry-derivative thermogravimetry (TGGTG) and FT-IR techniques. With a linear heat rate, the diagrams show three endothermic processes. RCOOK and K 2 CO 3  are produced at 330 and 467°C, respectively, according to FT-IR analysis.

Molecular Structure and Thermal Analysis of Potassium Hydrogenphthalate Monohydrate