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SmCl 3  reacts with equimolar amounts of K[(S)-C 5 H 4 CHPhCH 2 NMe 2 ] and Na[C 5 Me 5 ] yielding [(S)-C 5 H 4 CHPhCH 2 NMe 2 ](C 5 Me 5 )SmCl(1). The methylation of complex 1 with LiMe and the reactions of the known analogues of 1, [(S)-C 5 H 4 CHPhCH 2 NMe 2 ](C 5 Me 5 )LnCl (Ln = Y (2), Lu (3)) with LiCH 2 SiMe 3  afford [(S)-C 5 H 4 CHPhCH 2 NMe 2 ](C 5 Me 5 )SmMe (4) and [(S)-C 5 H 4 CHPhCH 2 NMe 2 ](C 5 Me 5 )LnCH 2 SiMe 3  (Ln = Y (5), Lu (6)), respectively. The reactions of ScCl 3  and LuCl 3  with 1 equivalent of K[(S)-C 5 H 4 CHPhCH 2 NMe 2 ] or K[C 5 H 4 CH 2 CH 2 NMe 2 ] followed by 2 equivalents of Me 3 SiCH 2 Li yield the complexes [(S)-C 5 H 4 CHPhCH 2 NMe 2 ] Ln(CH 2 SiMe 3 ) 2  (Ln = Sc (7a), Lu (7b)) or (C 5 H 4 CH 2 CH 2 NMe 2 )Ln(CH 2 SiMe 3 ) 2  (Ln = Sc (8a), Lu (8b)), respectively.

Organometallic Compounds of the Lanthanides 169. Lanthanidocene Complexes Containing Chiral Nitrogen-Functionalized Cyclopentadienyl Ligands