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Chloride abstraction, using AgPF 6 , from tri(1- cyclohepta-2,4,6-trienyl)phosphane platinum and palladium dichloride, [P]MCl 2  [M = Pt (1), Pd (2)], affords the complexes {[P]MCl}PF 6  [M = Pt (3), Pd (4)] in good yields. The central metal is coordinated by the chloro ligand, the phosphorus atom and by three η 2 -C=C units, one of each C 7 H 7  ring. This assignment of a highly symmetrical C 3v  structure is based on a consistent set of NMR data ( 1 H,  13 C,  31 P,  195 Pt NMR), in agreement with NMR data of the corresponding known neutral iridium and rhodium complexes [P]MCl [M = Ir (5), Rh (6)]. The chemical shift δ 103 Rh of 6 was determined, and a nearly linear relationship δ 195 Pt / δ 103 Rh was established.

zeitschrift für naturforschung b

Tri(1-cyclohepta-2,4,6-trienyl)- phosphane, P(C 7 H 7 ) 3 , as a Tripodal Tetradentate Ligand in Cationic, Five-coordinate Complexes of Platinum(II) and Palladium(II)