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The title compounds were prepared through reactions of Li 2 Nb 6 Cl 16  with the corresponding crown ethers in acetone. All three compounds were obtained as dark brown crystals. Their structures were solved with the means of single-crystal X-ray diffraction.

zeitschrift für naturforschung b

Synthesen, Kristallstrukturen und magnetische Eigenschaften von [Li(12-Krone-4) 2 ][Li(12-Krone-4)(OH 2 )] 2 [Nb 6 Cl 18 ], [Li(15-Krone-5) 2 (OH 2 )] 3 [Nb 6 Cl 18 ] und [(18-Krone-6) 2 (O 2 H 5 )] 3 [Nb 6 Cl 18 ] / Syntheses, Crystal Structures and Magnetic Behaviour of  [Li(12-Krone-4) 2 ][Li(12-Krone-4)(OH 2 )] 2 [Nb 6 Cl 18 ], [Li(15-Krone-5) 2 (OH 2 )] 3 [Nb 6 Cl 18 ] and [(18-Krone-6) 2 (O 2 H 5 )] 3 [Nb 6 Cl 18 ]