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Single crystals of [(TMEDA)LiCl] 2 ·  toluene (1) and [(MeCN) 2 LiCl] n  (2) can be obtained by dissolving LiCl in TMEDA or acetonitrile and crystallization (after addition of toluene for 1) at -30 °C. 1 is a dimer in the solid state while 2 is polymeric. 1 crystallizes in the space group I 2/a, Z = 4, with lattice dimensions at -90 °C: a = 1475.3(1), b=1112.7(2), c = 1615.0(2) pm, β = 103.44(1)°; Rx = 0.0739 with a disorder of the TMEDA ligand in two twist-positions. Crystals of 2 possess the space group Pbcm, Z = 4, with lattice dimensions at -80 °C: a = 1256.8(2), b = 775.2(1), c = 758.6(1) pm;R 1  = 0.0419.

Die Kristallstrukturen von [(TMEDA)LiCl] 2 ·Toluol und [(MeCN) 2 LiCl] n: The Crystal Structures of [(TMEDA)LiCl] 2 Toluene and [(MeCN) 2 LiCl] n