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[Si(N(CH 3 ) 2 ) 2 (NLiC(CH 3 ) 3 ) 2 ] 2  results from the reaction of silicon tetrachloride with excess terf-butylamine, followed by halogen substitution with LiN(CH 3 ) 2 , and treatment with n-butyllithium in hexane. The title compound, found to be dimeric in the solid state, was characterised by single crystal X-ray diffraction (triclinic, Pi , a = 10.208(2), b = 12.140(2), c = 15.658(3) Å , a = 79.02(3), ß = 82.80(3), γ = 67.19(3)°, Z = 2, C 24 H 60 Li 4 N 8 Si 2  ), and by solid state and solution NMR-spectroscopy and mass spectrometry.

zeitschrift für naturforschung b

Dimeres Di(N-lithium–tert–butylamino)bis(dimethylamino)silan - [Si(N(CH 3 ) 2 ) 2 (NLiC(CH 3 ) 3 ) 2 ] 2  – Darstellung und Kristallstruktur / Dimeric Di(N -lithio-tert-butylamino)bis(dimethylamino)silane - [Si(N(CH 3 ) 2 ) 2 (NLiC(CH 3 ) 3 ) 2 ] 2  – Synthesis und Crystal Structure