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By reduction of [B 6 Cl 5 (p-C 6 H 4  (NO 2 ))] 2-  with hydrazine in the presence of Raney nickel in dichlorom ethane solution the amino derivative [B 6 Cl 5 (p-C 6 H 4 (NH 2 )] 2- is formed. X -ray diffraction analysis has been performed on a single crystal of (Ph 4 P) 2 [B 6 Cl 5 (p-C 6 H 4 (NH 2 ] ·2CH 3 CN-0,5Et 2 O(triclinic, space group P1̅, a = 12.870(6), b = 12.9406(5), c = 35,870(7) Å , a = 91,63(4), ß = 93,22(7), γ = 98,04(8)°, Z = 2). The  11 B NMR spectrum is consistent with a monosubstituted B 6  cluster. The IR and R am an spectra exhibit characteristic BB, CH , CC, and NH vibrations, respectively.

zeitschrift für naturforschung b

Darstellung,  11 B-,  13 C-NMR- und Schwingungsspektren von Cs 2 [B 6 Cl 5 (p-C 6 H 4 (NI-I 2 ))] sowie Kristallstruktur von (Ph 4 P) 2 [B 6 Cl 5 (p-C 6 H 4 (NH 2 ))]· 2 CH 3 CN · 0,5 Et 2 O / Preparation,  11 B,  13 C NMR and Vibrational Spectra of Cs 2 [B 6 Cl 5 (p-C 6 H 4 (NH 2 ))] and Crystal Structure of (Ph 4 P) 2 [B 6 Cl 5 (p-C 6 H 4 (NH 2 ))]· 2CH 3 CN · 0.5 Et 2 O