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Cs[(CF 3 ) 3 BNH 2 ] reacts with CF 3 NO to form cesium trans-trifluoromethyldiazenido-tris(trifluoromethyl) borate Cs[(CF 3 ) 3 BN=NCF 3 ] (2), the structure of which has been investigated by single-crystal X-ray diffraction. The diazene nature of the anion is confirmed by the length of the N=N bond, 1.231(6) Å, and the size of the N-N-B angle, 115.5(4)° - the B-N bond length being 1.559(7) A. Compound 2 is hitherto the first diazenidoborate which has been fully characterized

A Diazenidoborate: Formation and Structure of Cs[(CF 3 ) 3 BN=NCF 3 ]