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Lanthanide, Carbacylamidophosphate The coordination compounds of the general formula Ln(NO 3 ) 3 (HL) 2 (H 2 O) 2  H 2 O , where Ln = La, Ce -Nd, Sm -Dy, HL = CCl 3 C(O)NHP(O)[N(CH 2 CH 2 ) 2 O] 2 , dimorpholido-N-tri-chloroacetylphosphorylamide, have been synthesized. The complexes were studied by IR,  1 H and  31 P NMR and UV-VIS absorption spectroscopies. X-ray diffraction analyses indicate that all synthesized compounds are isostructural. The crystal structure of Nd(NO 3 ) 3 (HL) 2 (H 2 O) 2  H 2 O was solved (monoclinic, a = 11.0467(3), b = 15.9080(5), c = 24.1921(7) Å, β = 96.4080(10)°, space group P2 1 /n, V = 4224.7(2) Å 3 , Z = 4, R = 0.049, wR = 0.0915). The complex has a molecular structure. The monodentate neutral phosphorictriamide ligands are coordinated to the metal atom via the phosphoryl oxygen atom. The coordination polyhedron of Nd is a sphenocorona; C.N. = 10(60[NO 3  - ], 20[HL], 20[H 2 O]).

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Coordination Compounds of Lanthanide Nitrates with Dimorpholido-N-trichloroacetylphosphorylamide. The Structure of Di(dimorpholido-N-trichloroacetylphosphorylamide)- diaqua Neodymium(III)trinitrate