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Bridged N-thiocarbamoyl substituted bis-benzamidines (C 2 H 5 ) 2 N-C(S)-N=C(Ph)-NH-R-NH-C(Ph)=N-C(S)-N(C 2 H 5 ) 2  with different moieties R (H 2 L 1  : R = diphenylmethane-2,2'-diyl, H 2  L 2 : R = diphenylmethane-3,3'-diyl, and H 2 L 3 : R = diphenylmethane-4,4'-diyl) were synthe­sized by the reaction of N-(thiocarbamoyl)benzimidoyl chlorides with diamines. These quadri­ dentate ligands form neutral mononuclear (CuL 1 ), dinuclear (Cu 2 L 3  2 ) and trinuclear (Cu 3 L 2  3 ) copper(II) chelates in dependence of the different bridging unit in the ligands. The compounds were characterized by NMR, IR, EPR and XPS spectroscopy and FAB mass spectrometry. The molecular structures of the ligand H 2 L 3  and the complex CuL 1  have been determined by X-ray methods.

zeitschrift für naturforschung b

Vierzähnige Benzamidin-Liganden in ein-und mehrkemigen Kupfer(II)-Komplexen / Quadridentate Benzamidine Ligands in Mono-and Oligonuclear Copper(II) Complexes