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Reaction of OsCl 3 , with pentamethylcyclopentadiene in ethanol in air yields the ionic osmium( IV) compound [Cp* 2 OsCl] 2 [OsCl 6 ] which has been identified structurally and by vibrational spectroscopy. Under comparable conditions the RuCl 3  homologue yields the ruthenium( III) compound [Cp*RuCl 2 ] 2 , illustrating the more facile oxidation of the 5d element to the tetravalent state

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Characterization of the Inorganic/Organometallic Osmium(IV) Compound [Cp 2  Os IV Cl] 2  [Os IV Cl 6 ] as Formed by the Reaction of OSCI 3  with Pentamethylcyclopentadiene in Air