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9-Trimethylsilyl- and 9-trimethylgermyl substituted derivatives of 1-(9-fluorenyl)germatranes C 13 H 8 (R)Ge(OCH 2 CH 2 ) 3 N (1 - 3) (1: R = H; 2: R = Me 3 Si; 3: R = Me 3 Ge) were prepared by the reaction of 9-tribromogermyl derivatives of fluorene C 13 H 8 (R)GeBr 3  (4 - 6) with N(CH 2 CH 2 OSnAlk 3 ) 3  (7: Alk = Et; 8: Alk = Bu). 1-(9-Trimethylstannyl- 9-fluorenyl)germatrane (14) was synthesised by the reaction o f the germatrane (1) with Me 3 SnNMe 2  . Formulas and structures were established by elemental analyses, ( 1 H,  13 C) NMR spectroscopy and mass spectrometry; crystal structures of 2 and 14 are reported.

9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)- germatranes. Synthesis, Characterisation, and Crystal Structures