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Single crystals of MesSn(Cl)Me 2  (1) and Mes 2 SnCl 2  (2) were obtained by the reactions of MesGaCl 2  with Me 3 SnF and Mes 3 SnF, respectively. 1 and 2 are monomeric molecules in the solid state. 1: space group P2 1 /n, Z = 4. lattice dimensions at -70°C: a = 1202,3(1), b = 739,1(1), c = 1441,3(1) pm , β = 102,71(1)°, R 1  = 0,0469; 2: space group Pbcn, Z = 4, lattice dimensions at -50°C: a = 1107,0(2), b = 949,9(1), c = 1729,8(2) pm, R 1 = 0,049.

Die Kristallstrukturen von MesSn(Cl)Me 2 und Mes 2 SnCl 2 / The Crystal Structures of MesSn(Cl)Me 2 and Mes 2 SnCl 2