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The reaction of [(Ph 3 As)AuCl] with Ag 2 O in the presence of NaBF 4  in tetrahydrofuran affords three products, identified as [(Ph 3 As) 4 Au]BF 4  (40.3%), [(Ph 3 As) 2 Au]BF 4  (16.4%) and {[(Ph 3 As)Au] 3 O}BF 4  (17.3%). The properties of the main product agree well with recent literature data. The other two compounds are new and have been identified by their analytical, spectroscopic, and crystallographic data. The structures are isomorphous with those of the analogous Ph 3 P complexes. Variations in the stabilities are discussed in terms of kinetic and thermodynamic effects.

(Triphenylarsine)gold(I) Complexes: Synthesis of an Oxonium Salt and Redistribution of the Arsine Ligands