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Single crystals of (Mn 2.4 Cu 0.6 )TeO 6  (I), Ba 2 MnTeO 6  (II) and Pb(Mn 0.5 Te 0.5 )O 3  (III) have been prepared by crystallization from fluxes. X-ray investigations led to rhombohedric symmetry (I): R3̄, (II): R3̄m with the trigonal lattice constants (I): a = 8.826(1), c = 10.687(2) Å, Z = 2. (II): a = 5.817(8), c = 14.244(3) Å, Z = 3. Compound (III) crystallizes with cubic symmetry P43̄m, a = 4.045(3) Å, Z = 1. (I) is the first example of a manganese(II) tellurate and belongs to the structure type of A 3 XO 6  compounds like (Mn 2 In)SbO 6 , Mn 3 WO 6  and Ca 3 UO 6 . (II) exemplifies an ordered and (III) a disordered variation of the perovskites.

zeitschrift für naturforschung b

Zur Kristallchemie von Telluraten mit Mn 2+  im kationischen und anionischen Teil der Kristallstruktur: (Mn 2,4 Cu 0,6 )TeO 6 , Ba 2 MnTeO 6  und Pb(Mn 0,5 Te 0,5  )O 3  / On the Crystal Chemistry of Tellurates Containing Mn 2+  in the Cationic and Anionic Part of the Crystal Structure: (Mn 2,4 Cu 0,6 )TeO 6 , Ba 2 MnTeO 6  and Pb(Mn 0,5 Te 0,5 )O 3