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By treatment of [PtCl 6 ] 2-  with an excess of SCN –  in aqueous solution [Pt(SCN) 6 ] 2-  is formed. The X-ray structure determination on a single crystal of [Py 2 CH 2 ][Pt(SCN) 6 ] (orthor-hombic, space group Pna2 1 , a = 15.5084(9), b = 11.8444(11), c = 13.2830(9)Å, Z = 4) shows, that the thiocyanate groups are exclusively S-coordinated with average Pt-S distances of 2.378 Å and Pt-S-C angles in the range from 103.1° to 108.1°. Based on the molecular parameters of the X-ray determination the low temperature (10 K) IR and Raman spectra have been assigned by normal coordinate analysis. The valence force constant is f d (PtS) = 1.62 mdyn/Å.

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Schwingungsspektren und Normalkoordinatenanalyse von Hexathiocyanatoplatinat(IV), Kristallstruktur von [Py 2 CH 2 ][Pt(SCN) 6 ] /  Vibrational Spectra and Normal Coordinate Analysis of Hexathiocyanatoplatinate(IV), Crystal Structure of [Py 2 CH 2 ][Pt(SCN) 6 ]