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The new macrocyclic dithiocyanatocuprate(I) complex [NH 4 (18-crown-6){Cu(NCS) 2 }] has been prepared using a direct method of interaction and characterized by X-ray crystallography (orthorhombic, space group Cmc2 1 , with a = 12.453(2), b = 21.650(4), c = 8.151(2) Å, V = 2197.6(8) Å 3 , Z = 4 , R1 (F) = 0.054; wR2(F 2 ) = 0.141 for 972 unique reflections with I &gt; 2σ(I) and R1(F) = 0.082; w/?2(F 2 ) = 0.210 for all 1098 unique reflections). The lattice comprises complex cations [NH 4 (18-crown-6)] +  and infinite polymeric anions [Cu(NCS) 2 ] -  of a one-dimensional zig-zag structure. The copper atoms adopt three-fold coordination [CuN 2 S] (Cu-N 1,89( 1), 1,90( 1) Å; Cu-S 2.278(4) Å).

Crystal Structure of an Ammonium Dithiocyanatocuprate(I) Complex with 18-Crown-6, [NH 4 (18-Crown-6){Cu(NCS) 2 }] Obtained from Zero Valent Metal