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The crystal structure of acetate acidium hexafluoroantimonate CH 3 C(OH) 2  + SbF 6  −  has been determined on single crystals with MoKα radiation at -83 °C. The structure is triclinic, space group P1̄, Z = 2, and the cell dimensions are a = 604.7(1), b = 692.3(3), c = 951.7(2) pm, α = 102.13(2)°, β = 106.53(2)°, γ = 99.27(2)°. In the CH 3 C(OH) 2  +  cation the C-C distance is 147.8(6) pm , the C -O distances are 125.1(6) and 129.1(5) pm. The SbF 6  −  anion is slightly distorted octahedral.

zeitschrift für naturforschung b

Kristallstruktur von Acetat-acidium- hexafluoroantimonat CH 3 C(OH) 2 SbF 6  Crystal Structure of Acetate Acidium Hexafluoroantimonate CH 3 C(OH) 2 SbF 6