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The phase diagram of the ternary system Ca/Mo/O has been determined. Powder samples of the ternary compounds CaMoO 4 , CaMoO 3 , CaMo 5 O 8 , Ca 16.5 Mo 13.5 O 40  and Ca 5.45 Mo 18 O 32  were prepared by solid state reactions. Rietveld analysis based on powder X-ray diffraction data shows that the compound CaMo 5 O 8  has monoclinic structure (P2 1 /c) with a = 7.549, b = 9.064, c = 9.974 Å, β = 110.04°. CaMo 5 O 8 , Ca 16.5 Mo 13.5 O 40  and Ca 5.45 Mo 18 O 32  are semiconductors over the temperature range 75 to 300 K.

zeitschrift für naturforschung b

Zum System Ca/Mo/O: Phasendiagramm, Synthese und Charakterisierung der ternären Verbindungen / On the System Ca/Mo/O: Phase Diagram, Synthesis and Characterization of Ternary Compounds