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Single crystals of the compounds SrZn(VO)(PO 4 ) 2  (I) and BaCd(VO)(PO 4 ) 2  (II) have been prepared by solid state reactions in evacuated quartz tubes. X-ray investigations confirmed orthorhombic symmetry, space group D 15  2h -Pbca, lattice constants a/b/c (I): 9.066(1)/9.012(1)/17.513(1) Å and (II); 8.838(4)/8.915(4)/19.374(9) Å, Z = 8. Initially assumed isotypies of (I) and (II) to BaZn(VO)(PO 4 ) 2  proved to be erroneous considering significant details of the connectivity of the ZnO 4  and PO 4  tetrahedra (I) and the coordination sphere of cadmium (II), respectively. The similarities and differences of the crystal chemistry relation to (I) and (II) are discussed with respect to BaZn(VO)(PO 4 ) 2 . The Coulomb terms of the lattice energies of vanadyl M 2 (VO)(PO 4 ) 2  and divanadyl M(VO) 2 (PO 4 ) 2  phosphates are shown.

zeitschrift für naturforschung b

SrZn(VO)(PO 4 ) 2  und BaCd(VO)(PO 4 ) 2 : Zum BaZn(VO)(PO 4 ) 2 -Typ verwandte, jedoch nicht isotype Vanadylphosphate / SrZn(VO)(PO 4 ) 2  and BaCd(VO)(PO 4 ) 2 : Vanadylphosphates Related but not Isotypic to the BaZn(VO)(PO 4  ) 2  Type