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Single crystals of the new compound CaNi(VO)(PO 4 ) 2  have been prepared by solid state reactions below the melting point of the oxide mixture in evacuated quartz tubes. X-ray investigations led to orthorhombic symmetry, space group D 2h  16 -Pnma, a =14.113(1), b =6.408(1), c = 7.364(1) Å, Z = 4. The crystal structure shows  1  ∞ [NiO 4 ] and  1  ∞ [VO 6 P 2 O 3 ] polyhedra chains closely related to analogous chains in the isotypic compound CdV 2 O(PO 4 ) 2 . The short V -O distance of 1.66 Å indicates a vanadyl group as the main difference to CdV 2 O(PO 4 ) 2 . The short O-O distance of 2,395 Å of the edge-sharing PO 4  tetrahedra and VO 6  octahedra is discussed.

zeitschrift für naturforschung b

Kurze O-O-Abstände einer gemeinsamen Polyederkante bei Verknüpfung von PO 4 -Tetraedern mit VO 6 -Oktaedern im Vanadyl-Orthophosphat CaNi(VO)(PO 4 ) 2  / Short O-O Distances in Edge Sharing PO 4  Tetrahedra and VO 6  Octahedra of the Vanadyl- Orthophosphate CaNi(VO)(PO 4 ) 2