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Two equivalents of N-lithio-N-trimethylsilyl-amino-9-borabicyclo[3.3.1]nonane (1) react with tin and lead dichloride by salt elimination to give the corresponding bis(amino)stannylene 2 and -plumbylene 3, respectively. The compounds 2 and 3 are monomers in solution and were characterized by  1 H,  13 C,  14 N,  29 Si,  119 Sn and  207 Pb NMR spectroscopy.

N-Boryl-Substituted Bis(amino)stannylenes and -plumbylenes