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Single crystals of PbCu 2 I 4· 2(CH 3 CN) are formed by reaction of Pbl 2  with Cul in acetonitril. The compound crystallizes in the mono­clinic space group C2/m; a = 1625.8(3), b = 436.6(1), c = 1025.8(2)pm; β = 94.77(3)°; V = 725.7 pm 3  10 6 ; Z = 2. The crystal structure is built up by chains of trans-edge sharing  1  ∞ [PbI 6/3 ] octahedra and corner sharing  1  ∞ [CuI 3/3 CH 3 CN)] tetra­hedra connected by common I-I edges.

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Notizen: Synthese und Strukturuntersuchungen von Iodocupraten(I), XVIII. Darstellung und Kristallstruktur von PbCu 2 I 4  ·2CH 3 CN/Synthesis and Structure Investigations of Iodocuprates(I), XVIII. Preparation and Crystal Structure of PbCu 2 I 4  ·  2 CH 3 CN