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Single crystals of I RbCd 4 V 3 O 12  and TlCd 4 V 3 O 12  II have been prepared by solid state reactions in closed iron tubes. The compounds crystallize closely related to the Johillerite structure in the space group C 6  2h - C2/c with I: a = 13.058(3); b - 13.528(3), c = 7 .0 6 0 (2 )Å , β = 114.88(2)°; II: a = 12.999(6), b = 13.527(7), c = 7.055(3) Å , β = 114.88(4)°, Z = 4. Special features are the loss of Cu 2+  in order to gain an additional Cd 2+  position. The crystal structure is discussed with respect to related compounds of the Johillerite type.

zeitschrift für naturforschung b

Zum Mineral Johillerit verwandte Oxovanadate RbCd 4 V 3 O 12  und TlCd 4 V 3 O 12  / Oxovanadates RbCd 4 V 3 O 12  and TlCd 4 V 3  O 12  Related to the Mineral Johillerite