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Single crystals of the new compound BaCa(VO)(PO 4 ) 2  have been prepared by solid state reactions below the melting point of the reactants in evacuated quartz tubes. X-ray investigations led to monoclinic symmetry, space group C 2h  5 -  P2 1 /c, a = 7.300(1), b = 7.053(1), c = 14.460(1) Å, β = 101,43(1)°, Z = 4. The crystal structure is characterized by layers of corner-and edge-connected PO 4  tetrahedra and VO 1+5  octahedra. There is an unusually short O(1)-O(4) distance in a VO 6  octahedron of 2.44 Å associated with the sharing of edges with PO 4  tetrahedra. The short V-O distance of 1.61 Å indicates a vanadyl group.

Kantenverknüpfte VO 6 -0ktaeder und PO 4 -Tetraeder in BaCa(VO)(PO 4 ) 2 / Edge-Connected VO 6 Octahedra and PO 4 Tetrahedra in BaCa(VO)(PO 4 ) 2