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Chloro-Cycloselenazenium Hexachloroanti-monate(V), Synthesis, Crystal Structure [Se 3 N 2 Cl] + SbCl 6  -  has been prepared as red crystals by the reaction of the nitride chloride Se 2 NCl 5  with antimony(III) chloride in dichloromethane. It was characterized by a crystal structure determination. Space group PI, Z = 2, 4396 observed unique reflections, R = 0.030. Lattice dimensions at -80 °C: a = 698.2, b = 699.7, c = 1510.5 pm, α = 89.45°, β = 86.18°, γ = 68.22°. The structure consists of two symmetry-independent cations and two symmetry independent anions, which differ only slightly from each other. The cations contain Se3N2 five-membered rings, which deviate very little from planarity as shown by fol­ ding angles of 14° and 18°. The Se-N bond distances are between 171.4 and 176.4 pm suggesting double-bond constituents.

Synthese und Kristallstruktur von [Se 3 N 2 Cl] + SbCl 6 - / Synthesis and Crystal Structure of [Se 3 N 2 Cl] + SbCl 6 -