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(NH 2 ) 2 P(S)N=P(NH 2 ) 3  has been prepared by a two step synthesis. Suitable single crystals were obtained from an acetonitrile solution in a temperature gradient between 60 °C and room temperature. The crystal structure of (NH 2 ) 2 P(S)N=P(NH 2 ) 3  has been determined by single crystal X-ray methods (P2 1 /c, a = 998.27(9) b = 762.78(8), c = 1007.70(15) pm, β = 107.340(7)°, Z = 4). In the crystal structure each hydrogen atom is subject to a hydrogen bond. Four N-H -N hydrogen bonding interactions per molecule build up a framework connecting two molecules in eight-membered rings. Each sulfur atom shows six distances N-H···S in the range of weak hydrogen bonding interactions.

zeitschrift für naturforschung b

Synthese, Kristallstruktur und Eigenschaften von 1,1,3,3,3-Pentaaminol- 1-thio-1 λ 5 ,3λ 5 -diphosphaz-2-en (NH 2 )2P(S)N=P(NH 2 ) 3  / Synthesis, Crystal Structure, and Properties of 1,1,3,3,3-Pentaam 1-thio-1 λ 5 ,3λ 5 -diphosphaz-2-en (NH 2 )2P(S)N=P(NH 2 ) 3