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Single crystals of (I) Rb 4 Cd(VO)(V 2 O 7 ) 2 Cl und Tl 4 Cd(VO)(V 2 O 7 ) 2 Cl have been prepared by flux techniques. The compounds were examined by X-ray analysis. They crystallize with tetragonal symmetry, space group C 1  4 -P4 with (I): a=9.142(1); c=5.525(1), (II): a=9.150(1), c=5.405(1) A, Z = 4. Both compound belong to the K 4 CuV 5 O 15 Cl-Type. V (l) forms V 2 O 7  double tetrahedra, connected by square V(2)O 5  pyramids and CdO 4 Cl 2  octahedra. The short V(2)-O distance indicates a vanadyl group.

zeitschrift für naturforschung b

Synthese und Röntgen-Strukturuntersuchung von Rb 4 Cd(VO)(V 2 O 7 ) 2 Cl und Tl 4 Cd(VO)(V 2 O 7 ) 2 Cl / Synthesis and X-Ray Structure Analysis of Rb 4 Cd(VO)(V 2 O 7 ) 2 Cl und Tl 4 Cd(VO)(V 2 O 7 ) 2 Cl