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On chloride abstraction from chloro-bis{1,2,4-tri(tert-butyl)cyclopentadienyl}bismut(III) (2 ) with aluminum trichloride the salt [{C 5 H 2 (CMe 3 ) 3  - 1,2,4} 2 Bi] +  AlCl 4  -  (1) has been obtained in good yield. The crystal structure of 1 shows a bismocenium cation with nearly parallel η 5  - cyclopentadienyl rings (10.2° inclination of the best planes) and only a slight bending of the Cp cent  -Bi-Cp cent  axis (172.9°).

zeitschrift für naturforschung b

Synthese und Kristallstruktur von Hexa(tert-butyl)bismocenium-tetrachloroaluminat / Synthesis and Crystal Structure of Hexa(tert-butyl)bismocenium Tetrachloroaluminate