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(CuI) 2 P 14  is a new adduct of copper iodide to a neutral phosphorus polymer. It is obtained by reaction of Cul and P red  at 400 °C. The compound crystallizes monoclinically, space group P2 1 /c (No. 14), a = 9.919(2), b = 9.718(2), c = 16.478(3) Å, β = 105.71(1)°, V = 1529.0(7) Å 3 , with Z = 4. The crystal structure was refined to R1 = 0.029 for 2680 reflections and 173 parameters. It contains a new polymeric phosphorus allotrope with the translational unit P 14  ±0  consisting of experimentally unknown [P12] groups which are linked by [P2] fragments. The phosphorus rods consist of five-and six-membered rings, and are coordinated only by copper atoms.

(CuI) 2 P 14 : ein neues Phosphorpolymer in einer Kupferhalogenid-Matrix /(CuI) 2 P 14 : a Novel Phosphorus Polymer in a Copper Halide Matrix