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By reaction of [B 6 H 7 ] -  with PhHg(CH 3 COO) in dichloromethane [Hg(η 3 -B 6 H 6 )Ph] -  is formed. The crystal structure of [PPh 4 ][Hg(η 3 -B 6 H 6 )Ph] has been determined by single crystal X-ray diffraction analysis; monoclinic space group P 2 1 /c with a = 9.567(5) Å, b = 22.213(5) Å, c = 14.296(5) Å, β = 94.484(5)°. The  11 B NMR spectrum exhibits a doublet at -9.9 ppm shifted to lower field as compared with [B 6 H 7 ] -  and the  199 Hg NMR spectrum a singlet at -74.5 ppm. In the IR and Raman spectra characteristic B-H vibrations are observed

zeitschrift für naturforschung b

Darstellung und spektroskopische Charakterisierung von (η 3 -Hexahydro-closo-hexaborato)phenylquecksilber(1-) [Hg(η 3 -B 6 H 6 )Ph] sowie Kristallstruktur von [PPh 4 ][Hg(η 3 -B 6 H 6 )Ph] / Preparation and Spectroscopic Characterization of (η 3 -Hexahydro-closo-hexaborato)phenylmercury(1 -) [Hg(η 3 -B 6 H 6 )Ph]- and Crystal Structure of [PPh 4 ][Hg(η 3 -B 6 H 6 )Ph]